Type: Techniques
Structural characterisation of solid materials and immobilised substances on solids.
It enables the analysis of very diverse materials:
- Soil, wood, cellulose
- Ceramic materials
- Polymers
- Polymorphs, glass, metal and alloys
- Porous materials such as zeolites and aluminosilicates
- Nanoparticles
- Studies on solid organometallic complexes.
Bruker Avance III 400 WB spectrometer, with ultrashielded widemouth magnet (89mm), 400 MHz (9.4T), with two RF channels and high power amplifiers for solid-state experiments.
- DVT 1H/BB probe. 4mm multinuclear probe with broadband channel (range frequency from 15N to 31P).
- DVT 1H/BB Probe. 7mm multinuclear probe, with 1H channel and broadband channel with range frequency from 15N to 31P.
- 2H lock channel for observing liquids.
PA BBOF Probe. 5mm direct multinuclear probe with broadband channel (range frequency from 15N to 31P) and additional observation of 19F.
Acquisition of MAS and CPMAS-type (Cross Polarization under Magical Angle Spinning) spectra at controlled temperatures, with a rotational speed of up to 10.000 rpm
Observation of various cores of interest in solid compounds: 9Si, 13C, 31P, 11B, 27Al, etc.
High-resolution 1D and 2D NMR experiments for the structure elucidation of molecules of chemical origin.
Buerau Veritas Certificate ISO9001
10/1/2020 to 2023
