Type: Techniques
Small molecule structure elucidation: elucidation of connectivity, stereochemical configuration and conformation.
Structural characterisation of nanoparticles and their interactions with substrates.
Mobility studies and molecular dynamics.
Monitoring of chemical processes: kinetics.
Determination of association and molecular interaction processes.
Studies at variable temperatures.
Mixture analysis, component quantification and determination.
Studies on molecular dissemination, size and mobility.
Studies on chemical reaction mechanisms, characterisation of reaction intermediates, acquisition of kinetic and thermodynamic reaction parameters.
Studies on molecular interactions, association processes determination and host-guest affinity molecular interaction, enzyme-substrate molecular recognition.
Bruker Neo500 spectrometer, with a 500 MHz Bruker (11.7 T) standard mouth (54mm) shielded magnet and two radio frequency channels, a magnetic field gradients unit and the following accessories:
- BBOF Plus ATM.1H/BB/19F direct multinuclear probe (5mm) with field gradients on the z-axis and automatic frequency control. 1H channel, wideband channel (5N to 31P and direct observation of 19F).
- BBI. 1H/BB/ inverse probe (5mm) with field gradients on the z-axis. Wideband channel frequency interval of 5N to 31P.
- SampleCase automatic changer with a 24-sample capacity.
- BCUII, accessory for air temperature control up to -40ºC.
- Liquid nitrogen evaporator for experiments at lower temperatures.
High-resolution 1D and 2D NMR experiments for the structure elucidation of molecules of chemical origin.
Recording of multinuclear NMR 1D spectra for samples in dissolution (selective excitation, decoupling, NOE, DEPT, HETNOE, etc.).
Homonuclear two-dimensional NMR spectrum acquisition (COSY, NOESY, TOCSY, ROESY) and heteronuclear inverse detection (HMQC, HSQC, HMBC).
Observation of a wide variety of magnetic cores: 19F, 195Pt, 133Cs, 11B, 31P, 6Li, 29Si, etc.
Studies on dissemination, kinetics and experiments at variable temperatures.
Buerau Veritas Certificate ISO9001
10/1/2020 to 2023
